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高压直流等离子氮化温度对316L不锈钢显微组织和磨损性能的影响

Temperature Effect on Microstructure and Wear Property of 316L Stainless Steel by High-Voltage DC Plasma Glow-Discharge Nitriding

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【作者】 黎桂江彭倩李聪王莹高见王均沈保罗

【Author】 LI GUI-Jiang1,PENG Qian 2,LI Cong 2,WANG Ying 2,GAO Jian 3,WANG Jun 1,Shen Bao-luo 1(1.College of Materials Science and Engineering,Sichuan University,Chengdu,610064,China;2.National Key Laboratory for Nuclear Fuel and Materials,Nuclear Power Institute of China,Chengdu,610041;3.Chengdu Tool Institute,610051)

【机构】 四川大学材料科学与工程学院中国核动力研究设计院核燃料及材料国家级重点实验室成都工具研究所四川大学材料科学与工程学院 成都610064四川成都610041四川新都610051成都610064

【摘要】 用高压直流辉光放电等离子方法对316LSS进行渗氮处理,研究了氮化温度对渗层的组织和性能的影响。利用XRD衍射仪、光学显微镜、表面显微硬度计和带能谱仪(EDS)的扫描电镜(SEM)分别分析渗氮层的相组成、厚度和显微结构、表面硬度、N和Cr原子的浓度。结果表明:当氮化温度350℃≤T≤400℃时,氮化层为单一的S相;温度为480℃时,S相衍射峰消失,仅剩CrN相;氮化后获得约为5~9μm的渗层;渗层深度和表面显微硬度随着温度的升高而增加。用环块式的方法评价磨损性能的结果表明:不锈钢表面的耐磨性提高一倍以上;未氮化的不锈钢主要存在粘着磨损、氧化磨损和磨粒磨损;等离子氮化的主要存在氧化磨损。

【Abstract】 By applying the different high-voltage DC plasma glow-discharge nitriding(DCPN) tem-peratures,the microstructure and wear resistance of the surface-nitrided 316L stainless steel were investigated.The phase composition,thickness,micro-hardness and element profile were examined by X-ray diffractometer,Optical microscopy,Hardness tester and EDS(Energy dispersive spectrometer),respectively.The results showed that a homogenous layer S-phase was produced between 350℃and 400℃ and a single layer CrN at 480℃.The nitrided layer depth was approximately 5~9μm.Both the thickness and the surface-hardness of the nitrided layer increased with the temperature increasing.It also revealed that the wear resistance of the DCPN stainless steel can be improved by one times or more.Wear of the untreated 316L was severe and character-ized by strong adhesion,wear,whilst wear of the DCPN-treated 316L was mild and dominated by oxidation wear.

  • 【文献出处】 核动力工程 ,Nuclear Power Engineering , 编辑部邮箱 ,2007年05期
  • 【分类号】TG142.15
  • 【被引频次】14
  • 【下载频次】202
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