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乳安颗粒质量控制的研究
Study on quality control for ruan granule
【摘要】 目的:制定乳安颗粒质量控制方法。方法:采用薄层色谱法对处方中的柴胡、当归、浙贝母、连翘、白术、茯苓、延胡索进行定性鉴别;采用高效液相色谱法对处方中白芍中的芍药苷进行含量测定。结果:芍药苷在0.16~1.04μg范围内呈良好的线性关系(r=0.9998).加样回收率为98.9%~101.6%。结论:本方法能对乳安颗粒进行定性、定量检测,结果准确可靠。
【Abstract】 Objective To establish the method for quality control of Ruan Granule.Method:Radix Bupleuri,Radix Angelicae Sinensis,Bulbus Fritillariae Thunbergii,Fructus Forsythiae,Rhizoma Atractylodis Macrocephalae,Poria, Rhizoma Corydalis were identified by TLC,and the content of Paeoniflorin in white Peony root was determined by HPLC.Result:Paeoniflorin showed a good linear relationship at a range of 0.16-1.04 μg,r=0.9998.The recov- ery was 98.9%-101.6%.Conclusion:The methods are accurate and reliable.
【关键词】 乳安颗粒;
定性鉴别;
芍药苷;
薄层色谱;
高效液相色谱;
【Key words】 Ruan granule; identification; paeoniflorin; TLC; HPLC;
【Key words】 Ruan granule; identification; paeoniflorin; TLC; HPLC;
- 【文献出处】 药物分析杂志 ,Chinese Journal of Pharmaceutical Analysis , 编辑部邮箱 ,2006年03期
- 【分类号】R286.0
- 【被引频次】2
- 【下载频次】82