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毛脉酸模药材质量标准研究

Criteria of quality control for root of Rumex gmelini

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【作者】 王振月左月明康毅华崔红花李瑞明

【Author】 WANG Zhen-yue, ZUO Yue-ming, KANG Yi-hua, CUI Hong-hua, LI Rui-ming (College of Pharmacy, Heilongjiang University of Traditional Chinese Medicine, Harbin 150040, China)

【机构】 黑龙江中医药大学药学院黑龙江中医药大学药学院 黑龙江哈尔滨150040黑龙江哈尔滨150040

【摘要】 目的制定毛脉酸模药材质量标准,为该药用植物资源的开发利用提供科学依据。方法生药学研究,浸出物测定法,灰分测定法,水分测定法,薄层色谱法及HPLC色谱法。结果对毛脉酸模的性状、显微特征进行了描述;对14个不同产地毛脉酸模的浸出物、总灰分、酸不溶性灰分和水分进行了测定;同时进行了薄层定性鉴别和HPLC色谱的定量研究。结论通过研究制定了毛脉酸模的质量控制标准。

【Abstract】 Objective To provide scientific basis for the utilization and development of Rumex gmelini by setting up the quality control criteria of R. gmelini. Methods The pharmacognostical methods were employed. The extract of R. gmelini was examined. Moisture and ash were determined. And the bioactive constituents were analyzed by TLC and HPLC. Results The morphological and histological characters of R. gmelini were observed. Content of extract, total ash, acid-insoluble ash, and moisture of 14 samples from different habitats were determined. The qualitative and quantitative analysis by TLC and RP-HPLC (DAD) were preformed, respectively. Conclusion The methods developed in this experiment can be used for the quality control of R. gmelini.

【关键词】 毛脉酸模质量标准TLCHPLC
【Key words】 the root of Rumex gmelini Turcz. ex Ledeb.quality criteriaTLCHPLC
【基金】 国家自然科学基金资助项目(30270156);黑龙江省科学技术计划项目(G00C202301)
  • 【文献出处】 中草药 ,Chinese Traditional and Herbal Drugs , 编辑部邮箱 ,2005年12期
  • 【分类号】R282.2
  • 【被引频次】17
  • 【下载频次】370
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