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反相高效液相色谱法测定妇炎消片中盐酸小檗碱含量

Determination of Berberine Hydrochloride Content in Fuyanxiao Tablets by RP-HPLC

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【作者】 赵为民仲崇林杨美林刘诗月

【Author】 ZHAO Wei-Min a, ZHONG Chong-Lin b, YANG Mei-Lin b, LIU Shi-Yue b ( aThe Affiliated Hospital of Changchun Traditional Chinese Medicine University,Changchun 130021;  bJilin Provincial Institute of Traditional Chinese Medicine and Materia Medica,Changchun)

【机构】 长春中医学院附属医院吉林省中医中药研究院吉林省中医中药研究院 长春130021长春长春

【Abstract】 An RP-HPLC method was used to determine the content of berberine hydrochloride in Fuyanxiao tablets on a Diamonsil C_ 18 column. The mobile phase was a CH_ 3CN/KH_ 2P0_ 4(volume ratio 30∶70) mixture of pH=3, and the average rate of recovery of berberine hydrochloricde was 98.18%, with a RSD of 0.92%( n=5). The method is simple and accurate,and can be used for the quality control in the production of Fuyanxiao tablet.

  • 【文献出处】 应用化学 ,Chinese Journal of Applied Chemistry , 编辑部邮箱 ,2005年06期
  • 【分类号】TQ461
  • 【下载频次】68
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