节点文献
常温下合成磷酸三苯酯的研究
Study on the Synthesis of Triphenyl Phosphate at Room Temperature
【摘要】 研究了常温下由苯酚钠悬胶体与三氯氧磷反应合成磷酸三苯酯的工艺条件,找到了一条比较好的合成方法.此方法具有操作方便、条件温和、反应时间短、能耗低、腐蚀小、污染少、产物纯、产率高等优点.
【Abstract】 Some technological conditions of the synthesis of triphenyl phosphate by the reaction of sodium phenolate and phosphorus oxychloride were studied, and a better process was found out. This method pro- vided several advantages such as easy operation, mild reaction conditions, short reaction time, low energy consumption, less corrosion, low contamination, high purity and high yield of product.
【关键词】 磷酸三苯酯;
苯酚钠悬胶体;
常温;
合成;
【Key words】 triphenyl phosphate; the suspensoid of sodium phenolate; normal temperature; synthesis;
【Key words】 triphenyl phosphate; the suspensoid of sodium phenolate; normal temperature; synthesis;
【基金】 国家自然科学基金(No.29872011);教育部高等学校青年骨干教师基金;河北省教育厅基金(No.990104)资助项目
- 【文献出处】 有机化学 ,Chinese Journal of Organic Chemistry , 编辑部邮箱 ,2005年05期
- 【分类号】TQ265.1
- 【被引频次】14
- 【下载频次】630