【摘要】 从易得原料百菌清1出发,经过氟交换、氨解、水解、脱羧和酰化反应,合成得到10个新的多卤代苯甲酰基脲类几丁质抑制剂衍生物,总收率为30%～50%.所有化合物经HNMR,HREIMS,IR光谱证实.对化合物进行了生物活1性筛选,结果表明该类化合物对粘虫和蚊幼虫均有一定的杀虫活性.更多还原

【Abstract】 Ten novel polyhalo benzoylphenylurea chitin inhibitor derivatives have been synthesized in over 30%～50% yields from readily available starting material chlorothalonil 1 via fluorine exchange, aminoly- sis, decarboxylation and acylation reactions. All products were characterized by H NMR, HREIMS and IR 1 spectra. Preliminary bioactive research showed that some of the synthesized compounds have the potential insecticidal activities against Mythimna separata and Culex pipiens pallens.更多还原