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表面修饰In纳米微粒的声化学法制备及结构表征

Preparation and Characteration of Surface Modified Indium Nanoparticles by Sonochemistry

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【作者】 李志伟陶小军程亚敏吴志申张治军党鸿辛

【Author】 LI Zhi-Wei1,2 TAO Xiao-Jun2 CHENG Ya-Ming2 WU Zhi-Shen2 ZHANG Zhi-Jun*,2 DANG Hong-Xin 1,2 (1State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Scienes, Lanzhou 730000) (2Laboratory for Special Functional Materials, Henan University, Kaifeng 475001) (3Graduate School of the Chinese Academy of Sciences, Beijing 100049)

【机构】 中国科学院兰州化学物理研究所,固体润滑国家重点实验室,河南省特种功能材料重点实验室,河南大学,河南省特种功能材料重点实验室,河南大学,河南省特种功能材料重点实验室,河南大学,河南省特种功能材料重点实验室,河南大学,中国科学院兰州化学物理研究所,固体润滑国家重点实验室 兰州73000河南省特种功能材料重点实验室,河南大学,开封475001中国科学院研究生院,北京100049,开封475001,开封475001,开封475001,开封475001,兰州73000

【Abstract】 Surface modified indium nanoparticles were prepared by a simple and rapid process from bulk indium via ultrasound dispersion. The morphology and structure of synthesized nanoparticles were characterized by TEM, XRD, XPS and FTIR. The results show that the morphology of indium nanoparticles is spherical and the structure of indium nanoparticles is the tetragonal phase. The surface of indium nanoparticles was coated by 2 ethyl hexanoic acid, which could almost hold back oxidation of the indium nanoparticles. In addition, the tribological property of indium nanoparticles as additives in oil was evaluated on a four-ball tester and the results show that indium nanoparticles exhibit good performance in wear.

【关键词】 In纳米微粒声化学制备摩擦学
【Key words】 indiumnanoparticlessonochemistrypreparationtribology
【基金】 科技部“863”纳米专项资助项目(No.2002AA302607);河南省科技厅攻关项目(No.0424270117)。
  • 【文献出处】 无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2005年08期
  • 【分类号】O614.372
  • 【被引频次】8
  • 【下载频次】144
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