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不同形态的α-Fe2O3纳米粉体的水热合成、表征及其磁性研究

Hydrothermal Synthesis,Characterization and Magnetic Studies on Various Morphological Hematite Nanopowders

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【作者】 景志红王燕吴世华

【Author】 JING Zhi-Hong1,2 WANG Yan1 WU Shi-Hua*,1(1Department of Chemistry,Nankai University,Tianjin 300071)(2Department of Chemistry,Qufu Normal University,Qufu 273165)

【机构】 南开大学化学学院南开大学化学学院 天津300071曲阜师范大学化学学院曲阜273165天津300071天津300071

【Abstract】 Four different hematite (-Fe2O3) nanopowders with various morphologi es have been synthesized in the presence of surfactant (HPC) via hydrothermal ro ute at 180 ℃, using four kinds of iron salts, Fe2(SO4)3, FeC2O4, FeSO4 and (NH4 )3Fe(C2O4)3, as precursor materials. The products were characterized by means of X-ray diffraction (XRD), transmission electron micrograph (TEM), Fourier transf orm infrared spectroscopy (FTIR) and magnetization measurements. The hysteresis measurements show that the products exhibit weak ferromagnetic property at room temperature. It is concluded that the different precursor materials and the pres ence of the surfactant are important factors that exert significant effects on t he morphologies and magnetic properties of the products.

【基金】 国家自然科学基金资助项目(No.20271028)
  • 【文献出处】 无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2005年01期
  • 【分类号】O614
  • 【被引频次】39
  • 【下载频次】596
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