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水热法制备氧化锌纳米棒
Preparation of ZnO nanorod by hydrothermal method
【摘要】 用水热法以聚丙烯酰胺(PAM)为添加剂制备了氧化锌单晶纳米棒,并通过X-射线衍射(XRD)、透射电镜(TEM)及红外光谱(IR)和紫外-可见吸收光谱(UV-Vis)等测试手段对所得产物的组成和形貌进行了研究.TEM结果表明,所得产物为六角纤锌矿型氧化锌,纳米棒沿C轴取向生长,粒径分布均匀,长度2.5~3.0μm.当改变反应的溶剂,纳米棒的结构形态发生了很大改变.对PAM的作用和溶剂的影响作了简要论述.
【Abstract】 Single ZnO nanorods have been prepared by favorable hydrothermal method with polyacrylamide(PAM) as additives.The samples are characterized by X-ray diffraction(XRD),transmission electron microscopy(TEM),infrared absorption spectra(IR),and UV-Visible absorption spectra(UV-Vis).TEM results show that the nanorods have wurtzite(hexagonal) structure with good crystal state.The nanorods are straight and uniformly elongated along the c axis and show well-defined crystallographic faces.The length is about 2.5~3.0 μm.The possible function of PAM and the effects of solvent conditions are discussed.
- 【文献出处】 山东大学学报(工学版) ,Journal of Shandong University (Engineering Science) , 编辑部邮箱 ,2005年06期
- 【分类号】O614.241
- 【被引频次】36
- 【下载频次】1743