节点文献
水热合成PbTiO3纳米线
Hydrothermal Synthesis of Lead Titanate Nanowires
【摘要】 采用水热法合成了纯钙钛矿钛酸铅纳米线.实验采用醋酸铅[Pb(AC)2.3H2O],钛酸四丁酯[Ti(OC4H9)4]为原料,氢氧化钠为矿化剂,研究了不同水热反应温度对产物物相及形貌的影响.当温度为200℃,反应48h,可以生成直径为10nm左右,长度在几百纳米到几微米之间的纯钙钛矿钛酸铅纳米线.
【Abstract】 Pure perovskite structure lead titanate(PT)nanowires were synthesized under hydrothermal conditions,using lead acetic and tetrabutyl titanate as the starting materials and NaOH served as a mineralizer. The effects of temperature on the morphology and crystallographic structure were discussed. The results show that PT nanowires of tetragonal perovskite with diameters about 10nm and length range from several hundreds to 5μm can be fabricated by hydrothermal method at 200℃ for 48 h.
【关键词】 水热法；
钙钛矿结构；
钛酸铅纳米线；
【Key words】 hydrothermal method； perovskite structure； lead titanate nanowires；
【Key words】 hydrothermal method； perovskite structure； lead titanate nanowires；
【基金】 国家自然科学基金(50272020);湖北省自然科学基金创新群体项目
- 【文献出处】 四川大学学报(自然科学版) ,Journal of Sichuan University (Natural Science Edition) , 编辑部邮箱 ,2005年S1期
- 【分类号】TB383;
- 【被引频次】9
- 【下载频次】295