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杀虫单铵的高效液相色谱分析方法
HPLC Analysis of Monosultap Ammonium
【摘要】 采用高效液相色谱法分析杀虫单铵。使用ODS反相柱和可变波长紫外检测器,以1.0mol/L磷酸二氢钾水溶液为流动相,外标法对杀虫单铵的有效成分进行定量分析。其标准偏差为1.35,变异系数为2.13%,平均回收率为99.9%。该方法操作简单,定量准确,与其它方法比较易于推广应用,适用于产品的常规分析和质控研究。
【Abstract】 An HPLC method was used to analyze monosultap ammonium. Quantitative analysis of the active ingredi-ent was conducted using an ODS reversed-phase column, a variable wavelength UV detector, potassium dihydrogenphosphate solution as the mobile phase, and an external standard. Standard deviation, coefficient of variation, andaverage recovery rate were 1.35, 2.13%, and 99.9%, respectively. The method is simple to conduct, quantitativelyaccurate, and should be relatively easy to recommend and implement on a large scale when compared with othermethods. The method is suitable for both routine conventional analysis as well as for quality control.
- 【文献出处】 农药 ,Pesticides , 编辑部邮箱 ,2005年08期
- 【分类号】TQ450.7
- 【被引频次】2
- 【下载频次】127