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杀虫单铵的高效液相色谱分析方法

HPLC Analysis of Monosultap Ammonium

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【作者】 赵云和; 曲明清; 张瑞明; 赵伟;

【Author】 ZHAO Yun-He1, QU Ming-Qing2, ZHANG Rui-Ming3, ZHAO Wei4(1Shenyang Agricultural University, Shenyang 110161, China; 2Jilin Agricultural University, Changchun 130118, China; 3SinopecJianghan Salt & Chemical Complex, Qianjiang 433121, China; 4Shenyang Cenkey Chemcal Co., Ltd. Shenyang 110021, China)

【机构】 沈阳农业大学; 吉林农业大学; 中国石化江汉油田分公司盐化工总厂; 沈阳新纪化学有限公司 沈阳110161; 长春130118; 湖北潜江433121; 沈阳110021;

【摘要】 采用高效液相色谱法分析杀虫单铵。使用ODS反相柱和可变波长紫外检测器,以1.0mol/L磷酸二氢钾水溶液为流动相,外标法对杀虫单铵的有效成分进行定量分析。其标准偏差为1.35,变异系数为2.13%,平均回收率为99.9%。该方法操作简单,定量准确,与其它方法比较易于推广应用,适用于产品的常规分析和质控研究。

【Abstract】 An HPLC method was used to analyze monosultap ammonium. Quantitative analysis of the active ingredi-ent was conducted using an ODS reversed-phase column, a variable wavelength UV detector, potassium dihydrogenphosphate solution as the mobile phase, and an external standard. Standard deviation, coefficient of variation, andaverage recovery rate were 1.35, 2.13%, and 99.9%, respectively. The method is simple to conduct, quantitativelyaccurate, and should be relatively easy to recommend and implement on a large scale when compared with othermethods. The method is suitable for both routine conventional analysis as well as for quality control.

【关键词】 杀虫单铵; 分析; 高效液相色谱;
【Key words】 monosultap ammonium; analysis; HPLC;
  • 【分类号】TQ450.7
  • 【被引频次】2
  • 【下载频次】127
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