节点文献
硅肥中有效硅含量的测定方法研究
Study on Test Method of Determining Available SiO2 Content in Silicon-containing Fertilizer
【摘要】 采用氟硅酸钾容量法对硅肥中测定有效硅含量的实验条件进行了研究。氟硅酸钾容量法能够准确、快速、简便测定硅肥中有效硅含量。推荐沉淀冷却时间应控制在30min以上;沉淀的洗涤温度应控制在15℃以下;滴定指示剂可选用酚酞;通过对氟硅酸钾分析纯的水解,验证此方法水解完全。
【Abstract】 The test conditions of determination method for available SiO2 content in silicon-containing fertilizer with potassium fluorosilicate volumetric analysis were studied.The available SiO2 content in silicon-containing fertilizer can be exactly determined with potassium fluorosilicate volumetric analysis. The recommendatory refrigerant time must be above 30 min ;the washing for deposit temperature must be controled under 15 degree;the indicator of titration shold be phenothalin.By the hydrolyzation of potassium fluorosilicate ,the hydrolyzation can be validated absolutely.
【关键词】 硅肥;
有效硅;
氟硅酸钾容量法;
测定方法;
【Key words】 Silicon-containing fertilizer; Available SiO2; Potassium fluorosilicate volumetric analysis; Analytical process;
【Key words】 Silicon-containing fertilizer; Available SiO2; Potassium fluorosilicate volumetric analysis; Analytical process;
- 【文献出处】 辽宁化工 ,Liaoning Chemical Industry , 编辑部邮箱 ,2005年05期
- 【分类号】TQ449
- 【被引频次】3
- 【下载频次】405