节点文献
3-二甲胺基-1,2-丙二醇的合成与表征
Synthesis and Characterization of 3-dimethylamino-1,2-propanediol
【摘要】 在碱的催化作用下,采用3-氯-1,2-丙二醇与二甲胺进行反应,合成了3-二甲胺基-1,2-丙二醇。采用红外光谱、元素分析、阿贝折射仪等对产物进行了表征,研究了配料比、碱的性质等因素对产率的影响。研究结果表明,产物为3-二甲胺基-1,2-丙二醇,且产率大于70%。
【Abstract】 3-dimethylamino-1,2-propanediol was synthesized from 3- ch loro-1, 2-propanediol and dimethylamine under the catalysis of alkali and then was characterized by IR,elemental analysis and abbe refractometer. The effects on the yield were also investigated, such as the molar ratio of 3-chloro-1, 2 -propanediol and dimethylamine, the properties of the alkali etc. The results s how that the product is 3-dimethylamino-1, 2-propanediol and the yield is hig her than 70%.
【关键词】 3-二甲胺基-1,2-丙二醇;
3-氯-1,2-丙二醇;
二甲胺;
【Key words】 3-dimethylamino-1,2-propanediol; 3-chloro-1,2- propanediol; dimethylamine;
【Key words】 3-dimethylamino-1,2-propanediol; 3-chloro-1,2- propanediol; dimethylamine;
- 【文献出处】 聚氨酯工业 ,Polyurethane Industry , 编辑部邮箱 ,2005年04期
- 【分类号】TQ223.162
- 【被引频次】3
- 【下载频次】183