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相转移催化合成乙酸异戊酯
Synthesis of isopentyl acetate by phase pransfer catalysis
【摘要】 利用相转移催化剂催化合成乙酸异戊酯,最佳反应条件:催化剂用量1g/0.1mol异戊醇,酸醇比2:1,反应时间100min,收率77.56%。实验证明,相转移催化合成对该酯化反应是高效,低成本和实用的方法。
【Abstract】 Use of CTMAB as phase transfer catalyst on the esterification of isopentyl acetate was studied. The optimized conditions are following: the weight of catalyst is 1g/mol iso-Amyl alcohol, the mole ratio of acid to alcohol is 2:1 and the reaction time is 100min.The yield was 77.56 %. Experiment results showed that phase transfer catalyst (CTMAB) is highly active catalyst for this reaction. It is an inexpensive and very practical method.
- 【文献出处】 化学工程师 ,Chemical Engineer , 编辑部邮箱 ,2005年08期
- 【分类号】TQ225.24
- 【被引频次】1
- 【下载频次】160