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气相色谱-质谱法测定卷烟烟气总粒相物中的游离乙酸
DETERMINATION OF FREE ACETIC ACID IN CIGARETTE SMOKE CONDENSATES BY GC-MS
【摘要】 以异丙醇为溶剂,壬醇为内标,采用气相色谱-质谱法分析了卷烟烟气总粒相物中的游离乙酸,乙酸测定结果的相对标准偏差小于1%,平均回收率为99.59%。
【Abstract】 The content of free acetic acid in cigarette smoke condensates was determined by GC-MS with isopropyl alcohol as the solvent and nonanol as the internal standard. RSD of the method was less than 1% and the average recovery of acetic acid was 99.59%.
【关键词】 卷烟烟气总粒相物;
乙酸;
气相色谱-质谱法;
测定;
【Key words】 cigarette smoke condensates; acetic acid; GC-MS; determination;
【Key words】 cigarette smoke condensates; acetic acid; GC-MS; determination;
- 【文献出处】 化学分析计量 ,Chemical Analysis and Meterage , 编辑部邮箱 ,2005年03期
- 【分类号】TS47
- 【被引频次】2
- 【下载频次】130