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卷烟烟气中多环芳烃的测定

THE DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS IN TOBACCO SMOKE

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【作者】 王进路新曹建平华兆哲杨占平曹建华陈坚

【Author】 WANG Jin 1,2 LU Xin 1,2 CAO Jian-ping 1 HUA Zhao-zhe 1,2 YANG Zhan-ping 3 CAO Jian-hua 3 CHEN Jian 1,2 (1 Key Laboratory of Industrial Biotechnology,Ministry of Education Southern Yangtze University; 2 Laboratory of Environmental Biotechnology, School of Biotechnology,Southern Yangtze University,Wuxi,214036; 3 Nantong Cellulose Fibers CO.,LTD.,Nantong,226008)

【机构】 江南大学工业生物技术教育部重点实验室江南大学工业生物技术教育部重点实验室南通醋酸纤维有限公司江南大学工业生物技术教育部重点实验室 江南大学生物工程学院环境生物技术研究室无锡214036江南大学生物工程学院环境生物技术研究室南通226008214036

【摘要】 卷烟烟气样品经环己烷超声提取、薄层色谱分离纯化后 ,再用毛细管气相色谱分析测定 结果表明 ,多环芳烃的回收率在 80 %以上 ,检测限在 8— 10 0 pg之间 ,本方法测定的每支卷烟主流烟气中多环芳烃的浓度在 8 9— 4 5 4 8ng·支 -1之间 壳聚糖改性醋纤滤嘴对卷烟烟气中多环芳烃有较好的截滤效果

【Abstract】 A method for determination of polycyclic aromatic hydrocarbons(PAHs) in tobacco mainstream smoke by thin-layer/gas chromatography was established. The samples were extracted ultrasonically with cyclane, purified by thin-layer chromatography and then determined by gas chromatography. It was found that the recoveries of the PAHs were above 80% and the detection limits were between 8—100 pg.The PAHs in tobacco mainstream smoke were analyzed and their concentrations were found to be 8.9—454.8 ng/cigarette.Cigarettes with cellulose acetate filters modified by chitosan were measured and the decrease rates of PAHs were compared with the unmodified ones.

【基金】 国家烟草专卖局科技成果开发计划项目 (合同号 :110 2 0 0 3 0 2 0 3 1)
  • 【文献出处】 环境化学 ,Environmental Chemistry , 编辑部邮箱 ,2005年01期
  • 【分类号】TS47
  • 【被引频次】26
  • 【下载频次】414
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