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微波消化石墨炉原子吸收法测定动物组织中的微量铝

Graphite Furnace Atomic Absorption Spectrometry Determination of Aluminium in Viscera with Microwave Digestion Technique

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【作者】 陈安宁刘继文谢锋吉玉碧何锦林谭红

【Author】 CHEN An-ning, LIU Ji-wen, XIE Feng, JI Yu-bi, HE Jin-lin ,TAN Hong (College of Chemical Engineering, Guizhou University, Guiyang 550003, China;Liupanshui City Environment Protection Bureau, Liupanshui, Liupanshui 553000, China;Guizhou Research Center of Physical Testing and Chemical Analysis, Guiyang 550002, China)

【机构】 贵州大学化学工程学院贵州省六盘水市环境监测站贵州省理化测试分析研究中心贵州省理化测试分析研究中心 贵州贵阳550003贵州六盘水553000贵州贵阳550003贵州贵阳550002

【摘要】 采用微波消化测定动物组织中微量的铝。先用硝酸高压溶解,然后用石墨炉原子吸收测定。方法的检出限0.91 ng/ml,线性范围0-1000 ng/ml,其回收率为95.1%-104.7%.该方法简化了对动物组织中铝测定的消化,精密度高,检出限低。

【Abstract】 Determination of aluminium in viscera is conducted by adopting microwave digestion technique. It is determined with nitric acid in a high - pressure microwave oven and then analyzed by graphite furnace atomic absorption spectrometry. The detection limit is 0. 91ng/ml,The calibration lines are linear in the range of 0-1000 ng/ml,and the recoveries of these materials range from 95. 1% to 104. 8% . The method is simple,accurate and low on the detection limit.

  • 【文献出处】 贵州工业大学学报(自然科学版) ,Journal of Guizhou University of Technology(Natural Science Edition) , 编辑部邮箱 ,2005年06期
  • 【分类号】X835
  • 【被引频次】2
  • 【下载频次】70
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