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红外光谱法研究盐酸丁咯地尔的热降解过程
IR-Spectroscopic Study on Thermal Degradation Process of Buflomedil Hydrochloride
【摘要】 本文采用傅里叶变换红外光谱、热重等多种分析方法,对盐酸丁咯地尔的热降解机理进行了较为详细的研究。实验结果表明盐酸丁咯地尔的热氧降解过程分为两个明显的阶段:一是脱盐酸、脱羧裂解,剩下苯环骨架结构;二是苯环骨架完全氧化裂解。通过对原药及其热氧降解中间产物的红外光谱分析,证实了以上的热氧降解历程。
【Abstract】 Infrared spectroscopy(IR) and thermal gravity(TG) techniques were applied to investigate the thermal degradation mechanism of Buflomedil Hydrochloride which was proved to be two distinct stages:in the first stage hydrochloric acid and carboxyl pyrolyzed from benzene frame;then benzene frame was thoroughly oxidized.
【关键词】 傅里叶变换红外光谱;
盐酸丁咯地尔;
热降解;
【Key words】 Infrared spectroscopy; Buflomedil Hydrochloride; thermal degradation;
【Key words】 Infrared spectroscopy; Buflomedil Hydrochloride; thermal degradation;
- 【文献出处】 光散射学报 ,Chinese Journal of Light Scattering , 编辑部邮箱 ,2005年04期
- 【分类号】O657.33;TQ460.7
- 【被引频次】1
- 【下载频次】90