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拉曼描述碳纳米管系统:缺陷探测,产物热处理,过程分析和催化剂(英文)

Raman Characterization for the Carbon Nanotubes Synthesis: Defects Determination, Product Thermal Treatment,Process Analysis and Catalyst Design

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【作者】 骞伟中郁鉴源陈凤恩魏飞王垚余皓宁国庆罗国华

【Author】 QIAN Wei-zhong~(*1), YU Jian-yuan~2, CHENG Feng-en~2, WEI Fei~1, WANG Yao~1, YU Hao~1, NING Guo-qing~1, LUO Guo-hua~1 (1. Department of Chemical Engineering, Tsinghua University, Beijing, China, 100084 2. Analysis center, Department of Chemistry, Tsinghua University, Beijing, China, 100084)

【机构】 清华大学化工系清华大学分析中心(化学系)清华大学化工系 北京100084北京100084北京100084

【摘要】 利用拉曼散射技术从多角度研究了碳纳米管合成系统。发现拉曼散射技术不仅可表征碳纳米材料本身的特性,而且可分析宏观的多壁碳纳米管与单壁碳纳米管的生长过程。针对不同的碳纳米材料的生长特性提出了催化剂与反应器设计及过程控制的研究方向。同时还发展了一种基于拉曼光谱法的定量测定单壁碳纳米管含量的方法。

【Abstract】 Raman scattering technique is used to study the carbon nanotube synthesis system. It is found that it not only favors the determination of the characteristics of carbon materials itself, but also is effective to analyze the growth process of multiwalled and single walled carbon nanotubes in macroscopic scale. And consequently the rational catalyst and reactor design and the proper process control method are proposed, considering the differences in the growth of different nanometer carbon materials. Meanwhile, a method for the quantitative determination of the purity of single walled carbon nanotubes is proposed based on the Raman scattering technique.

  • 【文献出处】 光散射学报 ,Chinese Journal of Light Scattering , 编辑部邮箱 ,2005年01期
  • 【分类号】TB383
  • 【被引频次】4
  • 【下载频次】244
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