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等离子热丝化学气相沉积金刚石膜工艺参数研究
Study on deposition parameter of diamond film prepared by plasma hot-filament chemical vapor deposition
【摘要】 采用等离子热丝化学气相沉积(PHFCVD)装置进行了金刚石薄膜的制备实验。实验条件为:氢气流量为200sccm,甲烷流量为2~12sccm,基体温度为700~900℃,偏压为0~400V,真空室压力为4kPa。通过实验得出了甲烷含量、基体温度和偏压对沉积金刚石膜的影响,并运用扫描电子显微镜(SEM)、原子力显微镜(AFM)和X射线衍射(XRD)等测试方法对金刚石薄膜进行了观察分析。
【Abstract】 Diamond films were prepared by plasma assistant hotfilament chemical vapor deposition when the flow rate of H2 was 200sccm,the flow rate of CH4 was 2~12sccm,the substrate temperature was 700~900℃,the bias voltage was 0~400V and the pressure was 4kPa.It was found the effect of the flow rate of methane,substrate temperature and bias voltage on the deposition of the diamond films.At the same time,the diamond films were investigated by SEM,AFM and XRD.
【关键词】 等离子;
热丝化学气相沉积;
金刚石薄膜;
【Key words】 plasma; hot filament chemical vapor deposition; diamond film;
【Key words】 plasma; hot filament chemical vapor deposition; diamond film;
【基金】 山东省自然科学基金资助项目(Y2001F10)
- 【文献出处】 功能材料 ,Journal of Functional Materials , 编辑部邮箱 ,2005年07期
- 【分类号】TB43;
- 【被引频次】7
- 【下载频次】177