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快速间隙式加料法制备单分散二氧化硅微球
Method for rapid synthesis of monodisperse silica spheres
【摘要】 应用快速间隙式加料法制备了单分散二氧化硅亚微米粒子。粒径可控,单分散性良好。该方法可在1h之内将113nm的种子SiO2粒子增长到429nm。本方法制得的二氧化硅粒子可以用来制备具有优良的光学性能的光子晶体膜。
【Abstract】 A new method for synthesizing monodisperse silica spheres was reported. By rapidly adding raw material into the reaction system step by step, the different-sized silica spheres with narrow diameter distribution were obtained. The advantage of this method is that the large spheres can be synthesized in a short time. These spheres were used for the construction of photonic crystal with good optical properties.
【关键词】 二氧化硅;
光子晶体;
正硅酸乙酯;
水解;
【Key words】 silica; photonic crystal; tetraethyl silicate; hydrolyzation;
【Key words】 silica; photonic crystal; tetraethyl silicate; hydrolyzation;
【基金】 国家科技攻关资助项目(No.2003BA310A20).
- 【文献出处】 电子显微学报 ,Journal of Chinese Electron Microscopy Society , 编辑部邮箱 ,2005年03期
- 【分类号】TN304.05
- 【被引频次】10
- 【下载频次】419