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纳米AgCl水溶胶的制备与表征

Preparation and characterization of nanosized AgCl hydrosol

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【作者】 董相廷冯秀丽王进贤闫景辉刘钟馨洪广言

【Author】 DONG Xiang-ting, FENG Xiu-li, WANG Jin-xian, YAN Jing-hui, LIU Zhong-xin, HONG Guang-yan (College of Materials and Chemical Engineering,Changchun University of Science and Technology, Changchun 130022, China ,Changchun Institute of Applied Chemistry, Academia Sinica,Changchun 130022, China)

【机构】 长春理工大学材料与化工学院中国科学院长春应用化学研究所 吉林长春130022吉林长春130022吉林长春130022

【摘要】 采用沉淀法制备了AgCl纳米粒子水溶胶,对制备水溶胶的条件进行了系统地研究.TEM分析表明,AgCl纳米粒子呈球形,粒径小于30nm,粒度分布均匀,无明显团聚现象;ED分析表明,AgCl纳米粒子为多晶结构,其中有少量的发育较好的单晶颗粒存在.

【Abstract】 The AgCl nanoparticles hydrosol was prepared by the precipitation method. The preparative conditions of nanosized AgCl hydrosol were discussed systematically. TEM photos showed that the AgCl nanoparticles were spherical in shape, the size was less than 30nm, particle size distribution was in narrow range, and no agglomerates were observed. ED images indicated that the AgCl nanoparticles were polycrystalline structure, and some of AgCl were monocrystalline particles.

【关键词】 AgAgCl纳米粒子水溶胶沉淀法
【Key words】 AgAgClnanoparticleshydrosolprecipitation method
【基金】 吉林省教育厅科研计划资助项目(200224)长春理工大学科研发展基金资助项目(YJJ2001-15)
  • 【文献出处】 材料科学与工艺 ,Material Science and Technology , 编辑部邮箱 ,2005年01期
  • 【分类号】O614.122
  • 【被引频次】13
  • 【下载频次】360
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