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碱型Mn3O4/Tm2O3复合纳米材料的制备及其催化性能
Preparation of Basic Mn3O4/Tm2O3 Nanoparticles and Effect of Catalyst
【摘要】 用溶胶-凝胶法制备 Mn3O4/Tm2O3复合纳米材料; 应用 X 射线粉末衍射仪(XRD), 透射电子显微镜(TEM), 红外光谱分析方法(FTIR)等手段对样品进行表征,得出纳米粒子为四方晶系,平均粒径为 38.0nm; 并研究了碱型 Mn3O4/Tm2O3 复合纳米材料对有机农药甲胺磷的催化增敏作用, 结果表明质量比 Mn:Tm=100:0.1 与在400℃下灼烧 2h 的纳米材料的催化增敏作用最佳.
【Abstract】 The Mn3O4/Tm2O3 and basic Mn3O4/Tm2O3 nanoparticles were prepared by a Sol-Gel method.The powder is characterized by XRD,TEM and FTIR,showing that the powder is Mn3O4 square crystalloid,and the average diameter is 30.8nm.The effect of catalyst were studied on the increase sensitivity of methamilophos, it was found out increase sensitivity best when mMn : mTm= 100.0 : 0.1and be calcinated under 400℃ for 2 h..
【关键词】 溶胶-凝胶法;
碱型;
纳米Mn3O4/Tm2O3;
甲胺磷;
催化;
增敏作用;
【Key words】 Sol-gel method; basicity; nano-Mn3O4/Tm2O3; methamidophos; catalyst; cincrease sensitivity impregnate;
【Key words】 Sol-gel method; basicity; nano-Mn3O4/Tm2O3; methamidophos; catalyst; cincrease sensitivity impregnate;
- 【文献出处】 漳州师范学院学报(自然科学版) ,Journal of ZhangZhou Teachers College , 编辑部邮箱 ,2004年04期
- 【分类号】TB383;O643.3
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