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荆条叶挥发油的气相色谱-质谱分析

Determination of the Volatile Oil Extracted From Leaves of Vitex negundo var. heterophylla Rehd.by Gas Chromatography-Mass Spectrometry

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【作者】 王发松任三香杨得坡朱长山陆慧宁

【Author】 WANG Fa-song, REN San-xiang, YANG De-po, ZHU Chang-shan, LU Hui-ning( School of Pharmaceutical Sciences, Zhongshan University, Guangzhou 510275, China; Instrumentation Analysis ( Research Center, Zhongshan University, Guangzhou 510275, China;Henan Agricultural University, Zhengzhou 450002, China)

【机构】 中山大学药学院中山大学测试中心河南农业大学农学院中山大学测试中心 广东广州 510275广东广州 510275河南郑州 450002广东广州 510275

【摘要】 利用气相色谱-质谱(GC/MS)联用技术分析荆条叶挥发油中的化学组成。结果表明:荆条叶挥发油中共分离出了36种组分,确定了29种成分的化学结构和相对含量,占总组分相对含量的94.68%。其中萜类及其衍生物22种,占89.13%。含量最高的成分是β-丁香烯(48.70%),其次是β-金合欢烯(15.52%)等。

【Abstract】 The volatile oil extracted from dried leaves of Vitex negundo var. heterophylla Rehd. was determinated by gas chromatography-mass spectrometry (GC/MS). Thre results showed thirty-six constituents in sample have been separated. Among which, the chemical structure and relative content of twenty-nine constituents were identified, the sum of their contents was 94. 68% of the total. The twenty-two constituents assigned to ter-penoids and their derivatives make up 89. 13% of the total volatile substances. The main component was β-Caryophyllene making up 48. 70% of the total, β-Farnesene making up 15.52%.

  • 【文献出处】 质谱学报 ,Journal of Chinese Mass Spectrometry Society , 编辑部邮箱 ,2004年01期
  • 【分类号】O657.63
  • 【被引频次】20
  • 【下载频次】210
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