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2-苯乙烯基喹啉染料的无溶剂微波合成
Solvent-Free Synthesis of Styryl Dyes with Quinoline Nucleus Using Microwave Irradiation
【摘要】 在微波促进无溶剂条件下 ,由 2 甲基喹啉与取代芳香醛在醋酐作用下合成了一系列 2 苯乙烯基喹啉染料 ,该法操作简便、收率高 .经元素分析 ,1HNMR ,MS ,IR和UV确证了产物的结构
【Abstract】 A series of styryl dyes with quinoline nucleus were conveniently synthesized by the reaction of 2-methylquinoline with aromatic aldehydes in the present of Ac 2O under solvent-free microwave irradiation with high yields. The products were identified by 1H NMR, IR, MS, UV-vis and elemental analysis.
【关键词】 微波辐射;
苯乙烯染料;
2-甲基喹啉;
芳香醛;
【Key words】 microwave irradiation; styryl dye; 2-methylquinoline; aromatic aldehyde;
【Key words】 microwave irradiation; styryl dye; 2-methylquinoline; aromatic aldehyde;
【基金】 陕西省教委科研专项基金 (No .0 2JK0 60 )资助项目
- 【文献出处】 有机化学 ,Chinese Journal of Organic Chemistry , 编辑部邮箱 ,2004年01期
- 【分类号】TQ615
- 【被引频次】24
- 【下载频次】242