节点文献
单分散纳米InVO4(正交相)的低温合成
Synthesis for Single Dispersing Nano-crystalline InVO4 (orthorhombic)abstract:at Low Temperature
【Abstract】 InVO 4 is a new developed visible light responding photocatalyst for water decompos ition,which is obtained by a solid - state reaction at high temperature traditionally.In this paper,pure InVO 4 nano - crystalline powder has been prepared by a hydrothermal process at low temper ature and was characterized by TEM,IR,and X - ray diffraction.Many factors such as pH value,reaction time and temperature have been investigated.It is found that the optimal conditions for the preparati on is:n InCl 3 ∶ n NaVO 3 =1 ∶ 2;temperature:150 ℃ ;Reaction time:4~8h;pH=7.9~8.0.And the experimental result shows that it is a convenient way to get single dispersing InVO 4 nano - crys - talline powder by flux in alkyl alcohol.
【基金】 国家自然科学基金项目(No.20133010,20073007,20273014);教育部科学技术重点项目(No.30361,JA02138);福建省自然科学基金重大项目(No.2003F004)。
- 【文献出处】 无机化学学报 ,Chinese Journal of Inorganic Chemistry , 编辑部邮箱 ,2004年02期
- 【分类号】O614
- 【被引频次】12
- 【下载频次】198