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ICP-AES法测定高、中、低碳锰铁中磷

Measurement on Content of P in High,Medium and Low Carbon Manganese Iron by ICP-AES Method

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【作者】 崔隽沈克齐郁

【Author】 CUI Juan,SHEN Ke,QI Yu (Technology and Quality Department of WISCO,Wuhan 430083,China)

【机构】 武钢技术质量部武钢技术质量部 湖北武汉430083湖北武汉430083湖北武汉430083

【摘要】 用等离子发射光谱法测定高、中、低碳锰铁合金中的磷元素 ,试样用少量硝酸和盐酸在加热条件下分解 ,经过系列试验 ,选择仪器的工作条件 ,进行测定 ,建立了一套分析方法 ,方法精密度RSD小于 5 % ,经对照分析 ,分析结果令人满意。本方法快速准确 ,精密度良好 ,完全可以满足生产需要。

【Abstract】 The phosphorous content in the high,medium and low carbon manganese iron alloy is measured up by ICP-AES method in which trace amount of nitric acid and hydrochloric acid is dissolved under the heating condition.The work conditions for the instruments are determined and a set of analytical method established through a series experiments.The accuracy of this process RSD is less than 5?% and satisfactory results are achieved by comparative analysis.This method is believed to be fast and accurate and can basically meet needs in actual production condition.

【关键词】 ICP-AES锰铁
【Key words】 ICP-AESmanganese ironP
  • 【分类号】TG115.33
  • 【被引频次】2
  • 【下载频次】91
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