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镍-碳化硅纳米复合电铸层的制备

Preparation of Compound Electroplate Layer of Nano Ni-SiC Particulate

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【作者】 张文峰朱荻薛玉君赵飞

【Author】 Zhang Wenfeng Zhu Di Xue Yujun Zhao Fei (Nanjing Aerospace and Austronautics University, Nanjing, China)

【机构】 南京航空航天大学南京航空航天大学

【摘要】 在应用电铸技术制备Ni SiC纳米复合材料的工艺中 ,分析了当镀液pH值、温度以及搅拌速度一定时 ,镀液中纳米SiC颗粒悬浮量和阴极电流密度对Ni SiC复合电铸层中纳米SiC复合量和电铸速率的影响。用SEM对纳米复合电铸层的表面形貌和组织成分进行了分析 ,同时探讨了纳米复合电铸层中SiC颗粒复合量对其显微硬度的影响。结果表明 ,Ni SiC纳米复合电铸层表面光滑平整 ,显微组织均匀、致密 ,显微硬度较纯镍镀层有明显提高。

【Abstract】 Effects of the amoutnt of suspending nano-SiC particulate and cathode current density in the electrolyte on nano-SiC particulate amount and electrolyte rate in Ni-SiC compound electrolyte layer were analyzed at a given pH value, temperature and stirring speed for nano-Ni-SiC composite preparation. The surface morphology and structural constituent in the electrolyte layer were observed by SEM. Effects of nano-SiC particulate amount in compound electrolyte layer on the micro-hardness were approached. The results showed that the nano Ni-SiC plating layer possessed smooth and even surface, uniform and sound microstructure as well as higher micro-hardness than single Ni plating layer.

【基金】 国家自然科学基金资助项目 (50 0 750 4 0 );国防基础研究基金资助项目 (J1 50 0E0 0 2 )
  • 【文献出处】 特种铸造及有色合金 ,Special Casting & Nonferrous Alloys , 编辑部邮箱 ,2004年05期
  • 【分类号】TB383
  • 【被引频次】29
  • 【下载频次】258
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