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杭白菊中酞酸酯类环境污染物的测定
Determination of Phthalic Acid Esters in White Chrysanthemum Tea
【摘要】 目的 了解杭白菊中酞酸酯的污染状况。方法 采用毛细管柱气相色谱 -质谱联用 (gaschromatography massspectrometry ,GC/MS)的选择离子检测 (selectedionmonitoringmode ,SIM )技术 ,结合有机溶剂回流提取、低温浓缩的前处理方法。结果 样品中邻苯二甲酸二丁酯 (di n butylphthalate,DBP)和邻苯二甲酸二异辛酯 (di 2 ethylhexylphthalate,DEHP)含量分别为 (2 0 .0 9± 1.2 1) μg/g和 (8.5 2± 0 .4 6 ) μg/g。 结论 杭白菊的部分产区已受到酞酸酯类环境污染物的污染 ,须尽快研究并采取消除此类污染的措施。
【Abstract】 Objective To find out the level of phthalic acid esters(PAEs)pollution in white chrysathemum tea from Tong Xiang,Zhejiang.Methods The selective ion monitoring mode(SIM) of capillary column gas chromatography-mass spectrometry(GC/MS)coupled with organic solvent extraction and low temperature concentration techniques were used.Results The content of di-n-bytyl phthalate(DBP) and di-(2-ethylhexyl) phthalate(DEHP)were 20.09±1.21 μg/g and 8.52±0.46 μg/g respectively.Conclusion The white chrysanthemum tea growing area mentioned was proposed having been polluted by phthalic acid esters.The measures against this pollution must be investigated in order to take immediate measure.
【Key words】 white chrysanthemum tea; phthalic acid esters; gas chromatography-mass spectrometry; selective ion monitoring;
- 【文献出处】 同济大学学报(医学版) ,Journal of Tongji University (Medical Science) , 编辑部邮箱 ,2004年05期
- 【分类号】X835
- 【被引频次】17
- 【下载频次】178