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纳米X型沸石制备及其在镍废水吸附处理中的应用
Preparation of nano-meter x-zeolite and its application in nickel ion2+ treatment
【摘要】 用水热合成法合成了纳米级X型沸石分子筛,并采用透射电镜(TEM)和X射线衍射(XRD)进行了表征.研究了纳米X型沸石分子筛对Ni2+的吸附.考察了纳米X沸石分子筛用量、pH值、接触时间和温度对Ni2+的吸附去除的影响.结果表明,投加0.03g纳米X沸石分子筛用量在pH约为5.0,温度为25℃,吸附时间为5min,去除率达到98.2500.最大吸附量可达150mg/g.采用1mol/L的HCl能较完全洗脱纳米级X型沸石分子筛所吸附的Ni2+.表明纳米级X型沸石分子筛能循环使用,可应用于含镍废水的处理.
【Abstract】 Nano-meter x-zeolite was prepared by hydrothernal synthesis, and powders characterized by TEM and XRD.The absorption of nano-meter x-zeolite to Ni2+ was studied.Influence of dosage of nano-meter x-zeolite,pH value, time of contaction and temperature of wastewater on the absorption of Ni2+ was researched.Result shows that the ration of removal was 98.2500 when wastewter was keeping at a five pH value, and stirring for five minutes at 25 ℃ with the nano-meter x-zeolite dosage of 0.03 g.The max absorption was 150 mg/g. Ni2+ was absolutely eluted by 1 mol/L HCl solution.The nano-meter x-zeolite can be used circularly to treat Ni2+pollution in water.
【Key words】 hydrothernal synthesis; nano-meter x-zeolite; nickel ion2+; absorption;
- 【文献出处】 天津城市建设学院学报 ,Journal of Tianjin Institute of Urban Construction , 编辑部邮箱 ,2004年02期
- 【分类号】X703.1
- 【被引频次】7
- 【下载频次】270