节点文献
脑供氧颗粒剂中淫羊藿苷的RP-HPLC法测定
Determination of Icariin in Naogongyang Granule by RP-HPLC
【摘要】 目的:建立脑供氧颗粒剂中淫羊藿苷的含量测定方法。方法:应用RP-HPLC法测定,选用C18色谱柱,流动相为甲醇-水-冰醋酸(35∶25∶0.3),流速1.0mL/min,检测波长270nm,柱温为25℃。结果:线性关系良好,平均加样回收率为98.84%,RSD为1.83%(n=5)。结论:该方法简便准确,可用于脑供氧颗粒剂的质量控制。
【Abstract】 Objective:A determination method of Icariin in Naogongyang Granule was established. Method: The RP-HPLC was carried out on C18 column using methanol-water-acetic acid (35∶25∶0.3)as a mobile phase,the detecting wavelength was set at 270nm,the flow rate was 1.0mL·min-1,the column temperature was at 25℃. Result: The linear relationship was good,the average recovery was 98.84% and RSD was 1.83%( n =5). Conclusion: The method is simple,reliable and suitable for the quality control of Naogongyang Granule.
- 【文献出处】 特产研究 ,Special Wild Economic Animal and Plant Research , 编辑部邮箱 ,2004年01期
- 【分类号】R286.0
- 【下载频次】20