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浆态床一步法二甲醚合成技术研发
RESEARCH OF DME SYNTHESIS IN SLURRY REACTOR BY ONE STEP PROCESS
【摘要】 在实验室进行了对采用浆态一步法合成二甲醚研究 ,系统考察了各种工艺条件 ,如温度、压力、空速、氢碳比等参数对反应的影响 ,获得了最佳的操作条件 :温度 2 5 0℃~ 2 70℃ ,压力 4~ 5MPa ,空速 30 0 0~ 6 0 0 0ml/g .cat/h ,氢碳比 1∶1,在此基础上进行了 30 0 0t/a的中试实验 ,取得了满意的结果。
【Abstract】 DME synthesis in slurry reactor by one step process is studied in laboratory under various process conditions, such as temperature, pressure, space velocity, H/C ratio et al., on the reaction. The optimum operation conditions are obtained that the temperature is 250℃-270℃,the pressure is 4-5MPa, and the space velocity is 3000-6000ml/g.cat/h,the.H/C ratio is 1:1.Based on that 3000t/a pilot test is carried out and good resulus are achieved.
【关键词】 二甲醚;
合成技术;
一步法合成;
浆态床合成法;
天然气化工;
【Key words】 synthesis gas; slurry bed; one step process; DME; pilot tes;
【Key words】 synthesis gas; slurry bed; one step process; DME; pilot tes;
- 【文献出处】 石油与天然气化工 ,Chemical Engineering of Oil and Gas , 编辑部邮箱 ,2004年S1期
- 【分类号】TQ223
- 【被引频次】6
- 【下载频次】286