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热处理温度对ITO薄膜组织与光电性能的影响

Effect of Temperature of Heat Treatment on Microstructure and Optical-electrical Properties of ITO Thin Films

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【作者】 杨觉明张康虎余申卫余萍张海礁

【Author】 YANG Jue-ming~1, ZHANG kang-hu~2, YU shen-wei~2, YU Ping~1, ZHANG hai-jiao~1(1.School of Materials Science and Chemical Engneering,Xi′an Institute of Technology, Xi′an 710032, China; 2.CSIC No.12 Research institute,Xingping 713102,China)

【机构】 西安工业学院材料与化工学院中国船舶重工集团公司第十二研究所西安工业学院材料与化工学院 陕西西安710032陕西兴平713102陕西西安710032陕西西安710032

【摘要】 采用溶胶-凝胶工艺制备出纳米晶ITO透明导电薄膜。采用XRD和SEM分析了薄膜物相和显微形貌。采用面电阻仪和分光光度计测量了薄膜方阻和透光率。实验结果表明,随热处理温度升高,晶化趋于完整,组织逐渐均匀致密,晶粒有所长大,700℃热处理时薄膜完全晶化。另外,随热处理温度升高,方阻减小而透光率增加。经过700℃热处理,厚度400nm的ITO膜的方阻约300Ω/□,透光率>80%。

【Abstract】 The transparent conductive ITO thin films with less than 300Ω/□ of the sheet resistance and more than 80% of the visible tran smittance were prepared by a sol-gel process. The microstructure and phase of the films were analyzed by XRD and SEM. The sheet resistance and optical transmittance of the films were measured by the four-point probe method and spectrophotometer. The results show that the microstructure of the films homogenizes and crystallizes, the grains of the film are growth gradually, and optical transmittance of the films is also increase with increasing the temperature. On the other hand, the sheet resistance of the films is decrease with increasing the temperature.

【基金】 陕西省教育厅科技专项基金资助项目(02JK147)
  • 【文献出处】 热加工工艺 ,Hot Working Technology , 编辑部邮箱 ,2004年12期
  • 【分类号】TG156
  • 【被引频次】3
  • 【下载频次】238
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