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微量滴定法测定抗坏血酸(Vc)含量

Study on Micro-titration for Determination of Vitamin c Concentration

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【作者】 蔡凌霜徐昊张玉清

【Author】 CAI Ling-shuang,XU Hao,ZHANG Yu-qing (College of Chemistry and Molecular,Wuhan University,Wuhan 430072,China)

【机构】 武汉大学化学与分子科学学院武汉大学化学与分子科学学院 湖北武汉 430072湖北武汉 430072湖北武汉 430072

【摘要】 以常量、微量两种方法作对比,对Vc样品、番茄及市售某橙汁饮料中抗坏血酸(Vc)的含量进行了测定和讨论.其结果无显著性差异,t检f检均在允许范围之内,相对偏差小于5%.微量滴定的精度达到常量测定水平,可满足化学分析的要求.也证明了WD-COⅡ型微型滴定装置能满足微型定量分析化学实验的要求.

【Abstract】 The concentration of Vitamin C was determined in the Vitamin C tablet,jam of tomato and orange juice in the market by microtitration method with a novel device of micro-buret.The RSD is lower than 5%,which confirms to the erro requests of analytical chemistry.The parallel determination results were compared with those obtained from the conventional buret,which tested the reliability of the novel micro-buret.The t-examine value and F-examine value are in the allowed range.And the microtitration has no significant differeces compare with conventional titration and fulfills the requirements for chemical analysis.It illustrated that the WD-COⅡ titration apparatus can settle all the problems of the Microscale Analytical Chemical Experiment.

【关键词】 ML微型滴定抗坏血酸
【Key words】 ML(Microscale Chemistry)MicrotitrationVitamin C
  • 【文献出处】 内蒙古民族大学学报(自然科学版) ,Journal of Inner Mongolia University for Nationalities(Natural Sciences,Quarterly) , 编辑部邮箱 ,2004年05期
  • 【分类号】O656
  • 【被引频次】13
  • 【下载频次】462
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