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HPLC测定半夏泻心汤中盐酸小檗碱的含量

Determination of berberine hydrochloride in Banxia Xiexin mixture by HPLC

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【Author】 LIU Jie 1,WEI Yu-ming 1,ZHANG Wen-jie 1,LI Yan 1,LIU Jun-ying 2,REN Zheng-bin 3 (1.The Sencond Affiliated Hospital of Shenyang Medical College,Shenyang 110002,Liaoning,China;2.Jinzhou Deyisheng Medication Health Square Drugstore,LTD.Co,Jinzhou 121000,Liaoning,China;3.Shenyang Heping District No.1 Clinic,Shenyang 110003,Liaoning,China)

【机构】沈阳医学院附属第二医院药剂科；锦州市德怡生医药健康广场药店有限公司；沈阳市和平区第一门诊辽宁沈阳110002；辽宁沈阳110002；辽宁锦州121000；辽宁沈阳110003；

【摘要】建立一种HPLC测定半夏泻心汤中盐酸小檗碱含量的方法。用水∶乙腈 (1∶1) 10 0 0ml加入KH2 PO4,3 4克为流动相 ,检测波长 345nm ,平均回收率为 10 0 6 % (RDS - 0 84 %n - 5 )。结论 :该方法简便、快捷、准确更多还原

【Abstract】 A HPLC method was established for the determination of berberine hydrochloride in Banxia Xiexin mixture.Methods:The mobile phese was consisted of water:CH3CN(1∶1)1L added KH-2PO-4.The wavelength was at 345nm.Results:The average recoveries were 100.6%(RSD=0.84% n=5).Conclusion:The method was simple,rapid and accurate.更多还原

【关键词】盐酸小檗碱；高效液相色谱法；含量测定；
【Key words】 berberine hydrochloride； HPLC； contain determination；

【文献出处】辽宁中医杂志 ,Liaoning Journal of Traditional Chinese Medicine , 编辑部邮箱 ,2004年05期

【分类号】R2841
【被引频次】2
【下载频次】179

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