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超声波法从罗汉果渣中提取碱木质素的研究
STUDY ON ULTRASONIC EXTRACTION OF ALKALINE LIGNIN FROM MOMORDICA GROSVENORI S.FRUIT RESIDUES
【摘要】 在一般碱法提取罗汉果渣木质素的基础上,加入超声波处理,确定了其最佳提取工艺条件为:10g样品在碱浓度0.5mol/L、碱液用量30mL/g、超声波处理时间90min、水浴温度40℃、恒温时间2.5h,木质素的溶出率由5.04%提高到8.60%,提取率由4.91%提高到8.40%;提取物中木质素含量为罗汉果渣中木质素总含量的56.19%。测定了IR光谱图,并且通过粘度法比较了其相对分子质量。
【Abstract】 Compared with the traditional method to obtain lignin by alkali extraction from Momordica grosvenori (Swingle) fruit residues,ultrasonic extraction was used for the dewaxed samples with 0.5 mol /L KOH at 40 ℃ for (2.5 h).The optimum extraction technology was as follows:ultrasonic irradiation time 90 min,temperature 40 ℃,(constant) (temperature) time 2.5 h.Under this condition,the total dissolved lignin increased from 5.04% to 8.60%,and the (extraction) rate increased from 4.91% to 8.40%.The yield of lignin was 56.19%.IR and molecular weight (measurements) of the alkali-soluble lignins were carried out.
【Key words】 alkaline lignin; Momordica grosvenori Swingle fruit residues; ultrasonic wave;
- 【文献出处】 林产化学与工业 ,Chemistry & Industry of Forest Products , 编辑部邮箱 ,2004年04期
- 【分类号】TQ914
- 【被引频次】15
- 【下载频次】515