节点文献
柱上层析法提纯双马来酰亚胺
Purification of BMI by column chromatography
【摘要】 为制备高纯度的双马来酰亚胺 ,减少双马来酰亚胺单体中杂质对单体本身反应活性及其性能的影响 ,采用柱上层析法提纯粗双马来酰亚胺 ,经高效液相色谱分析纯度达99.61 % ;通过晶体结构分析研究了其晶体结构 ,分子式和分子结构透视图
【Abstract】 The impureties in bismaleimide(BMI)monomer have many bad effects on the reactivity of the monomer and properties of BMI resin.The BMI monomer is purified by column chromatography and its purity is99.61%(analysized by HPLC).A single crystal with a suitable size was used for X-ray diffraction study.the crystal structure and molecule structure orthodiagram of this monomer are presented in this paper.
【关键词】 柱上层析;
双马来酰亚胺;
高效液相色谱;
【Key words】 bismaleimide; column chromatography; high performance liquid chromatography; crystal structure;
【Key words】 bismaleimide; column chromatography; high performance liquid chromatography; crystal structure;
- 【文献出处】 绝缘材料 ,Insulating Materials , 编辑部邮箱 ,2004年03期
- 【分类号】TM215
- 【被引频次】2
- 【下载频次】127