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Fe-Mn-Si形状记忆合金应力诱发马氏体相变的X射线分析

X-ray Analysis for Stress-Induced Martensitic Transformation in Fe-Mn-Si Based Shape Memory Alloy

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【作者】 林成新谷南驹张建军刘庆锁

【Author】 LIN Cheng-xin 1, GU Nan-ju 2, ZHANG Jian-jun 2, Liu Qing-suo 3 (1. School of Mechanical Engineering, Hebei University of Technology, Tianjin 300130,China; 2. School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130,China; 3.School of Materials Science and Engineering,Tianjin University of Technology,Tianjin 300191,China)

【机构】 河北工业大学机械工程学院河北工业大学材料科学与工程学院天津理工大学材料科学与工程学院 天津300130天津300130天津300191

【摘要】 采用X射线衍射法对Fe 17Mn 5Si 10Cr 5Ni和Fe 17Mn 5Si 2Cr 2Ni 1V合金的应力诱发马氏体相变进行了定量的分析。研究结果表明 ,Fe 17Mn 5Si 10Cr 4Ni合金试样在室温下拉伸 ,当变形量约为6 %时 ,应力诱发ε马氏体的体积分数达最大值约 6 4 % ;在预变形量超过 5 %时 ,α′马氏体即开始出现且增加迅速 ;揭示在大变形下 ,Fe Mn Si合金中发生了应力诱发γ→ε→α′马氏体相变。Fe 17Mn 5Si 2Cr 2Ni 1V合金试样在室温拉伸时应力诱发ε马氏体量较Fe 17Mn 5Si 10Cr 4Ni合金更多 ,即使在预变形量超过 10 %时 ,也不出现α′马氏体。预变形温度降低 ,可促进应力诱发马氏体相变。

【Abstract】 The stress-induced martensitic transformation in Fe-17Mn-5Si-10Cr-4Ni and Fe-17Mn-5Si-2Cr-2Ni-1V shape memory alloys have been quantitatively analyzed by means of XRD analysis. It is found that in Fe-17Mn-10Cr-5Si-4Ni alloy, the volume fraction of stress induced ε martensite reaches its maximum value of about 64% under a tensile deformation of about 6% at room temperature. As pre-strain exceeds 5%,α′ martensite appears and grows quickly in the alloy. The results prove that the γ→ε→α′ martensitic transformation occurs in Fe-Mn-Si alloy under large deformation. The amount of stress-induced ε martensite in the Fe-17Mn-5Si-2Cr-2Ni-1V alloy deformed at room temperature is more than that in the Fe-17Mn-5Si-10Cr-4Ni alloy and no α′ martensite is observed even under a deformation more than 10%. The stress-induced martensitic transformation in Fe-Mn-Si based shape memory alloy can be enhanced by decreasing the deformation temperature.

【基金】 国家自然科学基金资助项目 (5980 1 0 0 5) ;河北省自然科学基金资助项目 (50 30 38)
  • 【文献出处】 材料热处理学报 ,Transactions of Materids and Heat Treatment , 编辑部邮箱 ,2004年03期
  • 【分类号】TG139.6;TG113
  • 【被引频次】11
  • 【下载频次】391
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