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Synthesis and Crystal Structure of Bis-{N- [2-(6-ethylpyridyl)]-salicylideneiminato} Cobalt(Ⅱ)

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【Author】 YANG Hai-Jiana WANG Hong-Genb SUN Wen-Huaa② a (State Key Laboratory of Engineering Plastics and the Center for Molecular Science, Institute of Chemistry, The Chinese Academy of Sciences, Beijing 100080, China) b (State Key Laboratory of Functional Polymer, Nankai University, Tianjin 300071, China)

【Abstract】 The title complex 1, C28H26CoN4O2, crystallizes in the triclinic system, space group P with a = 9.506(3), b = 9.506(3), c = 14.837(5) ? a = 106.397(5), b = 106.012(5), g = 91.889(6), V = 1217.7(7) 3, Z = 2, Dc =1.390 g/cm3, Mr = 509.46, F(000) = 530, m(MoKa) = 0.738 mm-1, the final R = 0.0359 and wR = 0.0951 for 4275 observed reflections with I > 2s(I). The complex adopts a distorted tetrahedral coordination sphere around the cobalt atom.更多还原

【关键词】 cobalt(Ⅱ) complex； crystal structure； tetrahedral coordination；
【Key words】 cobalt(Ⅱ) complex； crystal structure； tetrahedral coordination；

【基金】 This work was supported by the National Natural Science Foundation of China (No. 20272062)

【文献出处】结构化学 ,Chinese Journal of Structural Chemistry , 编辑部邮箱 ,2004年02期

【分类号】O627
【被引频次】3
【下载频次】27

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