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低温陈化法制备ε-Zn(OH)2晶体及其表征

Preparation and characterizatinon of ε-Zn(OH)2 crystals by aging at low temperature

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【作者】 李平张萍鲁彬贾振斌魏雨

【Author】 LI Ping~1,ZHANG Ping~2,LU Bin~1,JIA Zhen-bin~1,WEI Yu~(1*)(1.Department of Chemistry,Hebei Normal University,Shijiazhuang 050016,China;2.Shijiazhuang Teachers College,Shijiazhuang 050801,China)

【机构】 河北师范大学化学学院石家庄师范专科学校河北师范大学化学学院 河北 石家庄050016河北 石家庄050801河北 石家庄050016

【Abstract】 ε-Zn(OH)2 crystals with high thermal stability,well crystallinity and fine dispersity were prepared by aging at low temperatue from zinc nitrate and sodium hydroxide in aqueous solution. The crystal structure,morphology and thermal stability were characterized by Xray diffractometry,scanning electron microscopy and differential scanning calorimeter. The influences of reaction temperatures,mole ratios of zinc nitrate to sodium hydroxide and phase-inversion rates on the products were discussed in details.

【关键词】 ε-Zn(OH)2晶体制备低温陈化
【Key words】 ε-Zn(OH)2crystalpreparationaging at low temperature
【基金】 河北省自然科学基金资助课题(501115)
  • 【文献出处】 化学研究与应用 ,Chemical Research and Application , 编辑部邮箱 ,2004年01期
  • 【分类号】O782
  • 【被引频次】4
  • 【下载频次】190
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