【摘要】 用碳酸钠控制pH ,四丁基溴化胺为相转移催化剂 ,将氮芥苯甲酸与溴代乙酰糖 (溴代乙酰葡萄糖、溴代乙酰半乳糖、溴代乙酰乳糖 )反应 ,合成了 3个氮芥苯甲酸糖酯 ,经IR、1 HNMR确定了糖酯的结构和构型更多还原

【Abstract】 Three new glucosyl esters of p [N,N bis(2 chloroethyl)amino]benzoic acid were synthesized by the reaction of p [N,N bis(2 chloroethyl)amino]benzoic acid with O acetylglucopyranosyl bromide or O acetylgallactopyranosyl bromide, O acetyllactopyranosyl bromide in the presence of Bu 4NBr and Na 2CO 3.Their structures were identified by elemental analysis,IR,and 1HNMR .更多还原