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粉煤灰中微量有害元素砷的氢化物-原子荧光光谱法快速测定
Rapid Determination of Trace Arsenic in Fly Ash by Hydride Generation Atomic Fluorescence Spectrometry
【摘要】 采用王水分解试样 -氢化物发生原子荧光光谱法 (HG -AFS)测定粉煤灰中有害微量元素砷。方法回收率为 98 5 %~ 1 0 2 3 % ,相对标准偏差为 1 9%~ 4 8% ,该法具有快速、简便、灵敏、可测范围宽等优点 ,对探讨粉煤灰在农业土壤改良中的应用具有十分重要的意义
【Abstract】 The sample was dissolved in aqua vegia,then the content of arsenic was directly determined by HG-AFS.The method is quick,accurate,economical and has wide linearity range.The relative standard deviation was 1.9%~4.8% and the recovery is 98.5%~102.3%.The method has been applied to determination of the fly ash samples with satisfactory results.
【关键词】 氢化物发生;
原子荧光光谱法;
粉煤灰综合利用;
砷;
【Key words】 hydride generation; AFS; fly ash comprehensive utitilzation; arsenic;
【Key words】 hydride generation; AFS; fly ash comprehensive utitilzation; arsenic;
- 【文献出处】 广东微量元素科学 ,Trace Elements Science , 编辑部邮箱 ,2004年07期
- 【分类号】X773
- 【下载频次】86