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火焰原子发射光谱法测定枣汁饮料中钾和钠

Flame atomic emission spectrometry for measurement of potassium and sodium contents of jujube juice

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【作者】 王秀敏陈彦昌谷俊涛岳艳玲刘丽娟

【Author】 WANG Xiu-min, CHEN Yan-chang, GU Jun-tao, YUE Yan-ling and LIU Li-juan (College of Life Science, Agricultural University of Hebei, Baoding 071001), Fenxi Shiyanshi,2004

【机构】 河北农业大学生命科学学院河北农业大学生命科学学院 保定071001保定071001保定071001

【摘要】 建立了火焰原子发射光谱法测定枣汁饮料中钾和钠的方法。将样品直接喷入空气 乙炔火焰中测定,测定结果与湿法消化法一致。钾、钠的方法检出限分别为:0.0021μg mL和0.0032μg mL。相对标准偏差(RSD)范围分别为:0 27%~0.98%和0.37%~0.59%。且与火焰原子吸收法进行比较,结果表明,发射法略优于吸收法。而对西红柿叶标准样品(ESP 1)进行对照测定,测定值与标准值基本吻合。

【Abstract】 A method was established for determination of potassium and sodium contents in jujube drink by flame atomic emission spectrometry (FAES). The samples were injected into air-acetylene flame to test. The detection limits of K and Na were 0.0021 μg/mL and 0.0032 μg/mL, respectively, and the relative standard deviations (RSD) were 0.27%~0.98% and 0.37%~0.59%, respectively. Compared with the flame atomic absorption spectrometry (FAAS), the FAES method showed better results. The tomato leaf (ESP-1) standard samples were used to carry out the comparative test. The determined values of the standard samples were in agreement with the certified values.

【关键词】 火焰原子发射光谱法枣汁
【Key words】 FAESJujube drinkPotassiumSodium
  • 【文献出处】 分析试验室 ,Analytical Laboratory , 编辑部邮箱 ,2004年08期
  • 【分类号】O657.31
  • 【被引频次】12
  • 【下载频次】254
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