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流动注射化学发光法测定尼莫地平
Determination of Nimodipine by Flow Injection Chemiluminescence Method
【摘要】 利用尼莫地平对Ce Na2 SO3 化学发光体系的抑制作用 ,建立了流动注射 化学发光法测定尼莫地平的新方法。化学发光强度与尼莫地平浓度在 0 .5~ 90mg/L范围内呈线性关系 ,线性范围为 0 .5~ 10mg/L时 ,r =0 .9990 ;线性范围为 10~ 90mg/L时 ,r =0 .996 8。回收率在 98.3%~ 10 3.2 %范围内 ;检出限为 0 .0 85mg/L。
【Abstract】 Method for the determination of nimodipine, based on the inhibition of the chemiluminescence (CL) reaction between cerium(Ⅳ) and sulphite, has been developed. The CL intensity is proportional to the concentration of nimodipine in the range of 0.5~10 mg/L (r=0.9990) and 10~90 mg/L (r=0.9968) . The recovery is 98.3%~103.2%. The detection limit is 0.085 mg/L and relative standard deviation is 1 8%.
- 【文献出处】 分析化学 ,Chinese Journal of Analytical Chemistry , 编辑部邮箱 ,2004年03期
- 【分类号】O657.3
- 【被引频次】28
- 【下载频次】193