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A Novel Flow Injection Chemiluminescence System for the Determination of Reserpine

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【Author】 ZHUANG Hui-shengCollege of Environment Science and Engineering, DongHua University, Shanghai 250001WANG Qiong-eCollege of Chemistry and Chemical Engineering, DongHua University, Shanghai 250001WEI Qiao-huaFujian Institute of Research on Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002WU Yan-linEnvironment Protection Office of Qingpu, Shanghai 201700

【机构】 College of Environment Science and Engineering； DongHua University； Shanghai 250001； professor； College of Chemistry and Chemical Engineering； Shanghai 250001； Fujian Institute of Research on Structure of Matter； Chinese Academy of Sciences； Fuzhou 350002； Environment Protection Office of Qingpu； Shanghai 201700；

【Abstract】 A novel flow injection cheminescence (FICL) system for the determination of reserpine is presented in this paper. It is based on the CL reaction of reserpine, IO - 4 and H 2O 2 in H 2SO 4 medium. The CL intensity was correlated with concentration of reserpine in the range of 1.0×10 -6～1.0×10 -4 g/mL with a detection limit of 1.35×10 -7 g/ mL. The relative standard deviation is 2.63% for 11 measurements of 2×10 -5 g/mL reserpine standard solution. The method has been applied to the determination of reserpine in pharmaceutical preparations and the results are in good agreement with that of the standard method.更多还原

【关键词】 Reserpine； Flow Injection Chemiluminescence； Determination；
【Key words】 Reserpine； Flow Injection Chemiluminescence； Determination；

【文献出处】 Journal of DongHua University ,东华大学学报(英文版) , 编辑部邮箱 ,2004年06期

【分类号】TQ463
【下载频次】34

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