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纯Ti纳米结构表层的探讨
Investigation of Nanostructured Surface Layer of Pure Titanium
【摘要】 利用表面机械处理技术在纯钛表面制备出50 靘厚纳米表面层, 采用金相显微镜(OM)、透射电镜(TEM)研究了处理层的微观结构。随着应变增加,晶粒逐渐细化。晶粒的细化机制为:孪晶的形成和孪晶碰撞;孪晶转变成取向不同的片状晶;片状晶转变成含有位错的胞状晶、取向不同的小角度块状晶以及取向不同的多边形亚细晶;亚细晶和片状晶转变成纳米晶。微观结构观察证实了动态再结晶促使晶粒细化。
【Abstract】 A nanostructured surface layer up to 50 祄 thick of commercially pure titanium was produced by a surface mechanical treatment (SMT) technique. The microstructure features of the SMTed surface layer were investigated by cross-sectional OM and TEM. The grain refinement process with the increase of the strain in the surface layer involves: (1) formation of twins and intersection of twin systems, (2) transformation of twins into low disoriented lamellae, (3) division of lamellae into dislocation cells, low-angle disoriented blocks and then highly disoriented polygonal submicronic grains, (4) further fragmentation of submicronic polygonal grains or residual lamellae into randomly oriented nanograins. There is microstructural evidence that a rotation recrystallization mechanism is operative.
- 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2004年06期
- 【分类号】TB383
- 【被引频次】3
- 【下载频次】109