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纯Ti纳米结构表层的探讨

Investigation of Nanostructured Surface Layer of Pure Titanium

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【作者】 赵永庆朱康英

【Author】 Zhao Yongqing1, Zhu Kangying1,2 (1. Northwest Institute for Nonferrous Metal Research, Xian 710016, China) (2. LASMIS, University of Technology of Troyes, Troyes 10000, France)

【机构】 西北有色金属研究院,西北有色金属研究院 陕西西安710016,陕西西安710016University of Technology of Troyes,Troyes 10000,France

【摘要】 利用表面机械处理技术在纯钛表面制备出50 靘厚纳米表面层, 采用金相显微镜(OM)、透射电镜(TEM)研究了处理层的微观结构。随着应变增加,晶粒逐渐细化。晶粒的细化机制为:孪晶的形成和孪晶碰撞;孪晶转变成取向不同的片状晶;片状晶转变成含有位错的胞状晶、取向不同的小角度块状晶以及取向不同的多边形亚细晶;亚细晶和片状晶转变成纳米晶。微观结构观察证实了动态再结晶促使晶粒细化。

【Abstract】 A nanostructured surface layer up to 50 祄 thick of commercially pure titanium was produced by a surface mechanical treatment (SMT) technique. The microstructure features of the SMTed surface layer were investigated by cross-sectional OM and TEM. The grain refinement process with the increase of the strain in the surface layer involves: (1) formation of twins and intersection of twin systems, (2) transformation of twins into low disoriented lamellae, (3) division of lamellae into dislocation cells, low-angle disoriented blocks and then highly disoriented polygonal submicronic grains, (4) further fragmentation of submicronic polygonal grains or residual lamellae into randomly oriented nanograins. There is microstructural evidence that a rotation recrystallization mechanism is operative.

【关键词】 表面纳米微观结构
【Key words】 nanostructured surface layertitaniummicrostructure
  • 【文献出处】 稀有金属材料与工程 ,Rare Metal Materials and Engineering , 编辑部邮箱 ,2004年06期
  • 【分类号】TB383
  • 【被引频次】3
  • 【下载频次】109
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