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相转移催化合成乙酸异丁酯
Synthesis of iso-Butyl Acetate by Phase Transfer Catalysis
【摘要】 利用相转移催化剂催化合成乙酸异丁酯,最佳反应条件如下:催化剂用量0.5g/0.1mol异 丁醇,酸醇比1.2:1,反应时间100分钟,收率77.36%。实验证明,相转移催化对该酯化反应是高 效、低成本和实用的合成方法。
【Abstract】 Use of TBAB as phase tranfer catalyst on the esterification of iso-Butyl acetate was studied. The optimized conditions are following: the weight of catalyst is 0. 5g/0. 1mol iso-Butyl alcohol , the mole ratio of acid to alcohol is 1. 2: 1 and the reaction time is 100min. The chemical yield was 79. 51%. Experiment results showed that phase transfer catalyst (TBAB) is highly active catalyst for this reaction. It is an inexpensive and very practical methed.
- 【文献出处】 长春师范学院学报 ,Journal of Changchun Teachers College , 编辑部邮箱 ,2004年02期
- 【分类号】O623
- 【下载频次】171