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壳聚糖硫酸盐催化对羟基苯甲酸酯合成的研究

Study on Catalytic Synthesis of Butyl Pphdroxybenzoate with Chitosan Sulfate

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【作者】 陈红祖峰洪莲

【Author】 CHEN Hong, ZU Feng, HONG Lian(Chemistry and Material Engineering Dept. of Hefei College, Hefei 230022, China)

【机构】 合肥学院化学与材料工程系合肥学院化学与材料工程系 安徽合肥 230022安徽合肥 230022安徽合肥 230022

【摘要】 本文研究了制备壳聚糖硫酸盐催化剂的相关影响因素,考察壳聚糖硫酸盐催化活性和稳定性,并用其催化合成对羟基苯甲酸丁酯。重点讨论催化剂用量,酸醇量比和反应时间对酯化率的影响,确定了较佳的反应条件。

【Abstract】 The preparation of chitosan sulfate and its main influential factors have been studied including its catalytic reaction and stability in some esterfations, and ethyl-hdroxybenzoate has been catalytically synthesized with chitosan sulfate. The reaction condition of-phydroxybenzoic acid with nbutyl alcohol by using chitosan sulfate as catalyst has been dealt with, and influences of amount of catalyst, the molar ration of alcohol toacid and reaction time that effects the esterifation have been mainly discussed.

  • 【文献出处】 安庆师范学院学报(自然科学版) ,Journal of Anqing Teachers College(Natural Science Edition) , 编辑部邮箱 ,2004年04期
  • 【分类号】O643.3;O625
  • 【被引频次】6
  • 【下载频次】208
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