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用热分析技术评价小麦新鲜度的研究

Evaluation of Wheat Freshness By Thermal Analysis Techniques

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【作者】 展海军范璐周展明周惠明

【Author】 Zhan Haijun, Fan Lu, Zhou Zhanming, Zhou Huiming( Chemistry and Chemical Engineering Department, Zhengzhou Institute of Technology, Zhengzhou 450052, China) (School of Food Science,Southern Yangtze University, Wuxi 214036,China)

【机构】 郑州工程学院化学化工系江南大学食品学院 郑州450052郑州450052无锡214036

【摘要】 本文利用热分析技术(TG、DSC、DMA)对小麦储藏过程中生物大分子物质的变化情况进行了探讨。TG法主要了解小麦的热稳定性,DSC法探索了小麦籽粒中大分子晶体区域的热量变化情况,测试结果表明:Tp随储藏时间的增加而增加,△H随储藏时间的增加而减少;DMA法讨论了小麦中非晶区大分子的热量变化情况,结果显示:Tg与储藏时间呈多项式的关系,相关系数为0.842;Te-To与储藏时间线性相关,相关系数0.956。通过测定Te-To,即可根据Y=-1.931X+116.5算出小麦储藏时间,进而评价其新鲜度。

【Abstract】 The change of biomacronolecule in wheat during storage was investigated by means of thermal analysis techniques, such as thermogravimetry ( TG) , differential nscaning calorimetry ( DSC) and dynamic mechanical analysis (DMA) . The thermal stability of wheat can be easily known by TG. The thermal properties of the biological polymer in wheat crystalline regions were revealed by DSC. The result showed that with the increase of wheat storage time their peak melting temperature (Tp) increased and the melting enthalpies (△H) decreased. Thermal characterization of amorphous or semi- crystalline biomaterimals in wheat were discussed by DMA. The result indicated the glass transition temperature (Tg) had amultinomial relationship with storage time(r = 0.842) ,and that the glass transition temperature range(Te - To) had a lineal relationship with storage time(r = 0.956) . The wheat freshness can be evaluated by calculation of the storage time according to the following equation: Y = -1.931X + 116.5.

【关键词】 小麦储藏时间新鲜度热分析
【Key words】 wheatstorage timefreshnessthermal analysis
  • 【文献出处】 中国粮油学报 ,Chinese Cereals and Oils Association , 编辑部邮箱 ,2003年01期
  • 【分类号】S375
  • 【被引频次】9
  • 【下载频次】171
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