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HPLC法测定脉络宁口服液中肉桂酸的含量
Determination of Cinnamic Acid in Mailuoning Oral Liquid by HPLC
【摘要】 目的 :测定脉络宁口服液中肉桂酸的含量 ,建立其定量检测方法。方法 :HPLC法。DikmaDimansilC1 8色谱柱 ;甲醇 0 1 %磷酸溶液 (55∶45)为流动相 ;检测波长 2 78nm ;外标法测定。结果 :平均回收率为 97 8% ,RSD =1 0 5 %。结论 :该方法简便、准确、可靠 ,适用于脉络宁口服液的定量检测
【Abstract】 Objective:To establish an HPLC method through determining the content of cinnamic acid in Mailuoning oral liquid Methods:HPLC was carried out with Dikma Dimansil C 18 column and methanol 0 1% phosphoric acid solution (55∶45) as the mobile phase The detection wavelength was 278 nm Results:The average recovery rate was 97 79%,RSD was 1 05% Conclusion:The method is simple,accurate and reliable It can be used for quantitative determination of Mailuoning oral liquid
【关键词】 HPLC;
脉络宁口服液;
肉桂酸;
玄参;
【Key words】 HPLC; Mailuoning oral liquid; Cinnamic acid; Radix scrophulariae;
【Key words】 HPLC; Mailuoning oral liquid; Cinnamic acid; Radix scrophulariae;
- 【文献出处】 江苏药学与临床研究 ,Jiangsu Pharmaceutical and Clinical Research , 编辑部邮箱 ,2003年01期
- 【分类号】R286.0
- 【被引频次】10
- 【下载频次】185